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KMID : 1059519970410120661
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Journal of the Korean Chemical Society
1997 Volume.41 No. 12 p.661 ~ p.665
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A Study on the Synthesis of Ammonium Dinitramide
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Chung Kyoo-Hyun
Sim Hyun-Ho
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Abstract
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Recently ADN was disclosed to replace AP or AN as a solid oxidizer. 3-N,N-Dinitraminopropanitrile, a key intermediate in the preparation of ADN, was synthesized from bis(2-cyanoethyl)amine by the sequence: nitration of bis(2-cyanoethyl)amine followed by decyanoethylation by base and the second nitration with NO2BF4. 3-N-Nitro-bis(2-cyanoethyl)amine could also be obtained by the oxidation of the corresponding N-nitroso compound.
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KEYWORD
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